Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane.

Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane. Research Abstract Details 

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Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane. Abstract Text:

Kai Du,Wuyou Fu,Ronghui Wei,Haibin Yang,Jing Xu,Lianxia Chang,Qingjiang Yu,Guangtian Zou,Kai Du,Wuyou Fu,Ronghui Wei,Haibin Yang,Jing Xu,Lianxia Chang,Qingjiang Yu,Guangtian Zou,

With ultrasonic irradiation as assistance, highly dispersed MoO(3) nanospheres were synthesized using silane coupling agent 3-mercaptopropyltrimethoxysilane HS-(CH(2))(3)Si(OCH(3))(3) (MPTS) as figuration agent. The results of X-ray powder diffractometer (XRD) showed that the precursor was hexagonal molybdenum oxide hydrate (MoO(3)0.55H(2)O). It was converted into orthorhombic MoO(3) after annealed at 400 degrees C for 2h. Transmission electron microscopy (TEM) showed that MoO(3).0.55H(2)O and MoO(3) nanoparticles were spherical with particle-size distribution of ca. 30-80nm and 25-75nm, respectively. Results indicated that MPTS and ultrasonic irradiation played important role in formation of highly dispersed MoO(3) nanospheres. X-ray photoelectron spectroscopy (XPS) was also adopted to confirm the growth mechanism. The possible cause of formation was based on dispersion function of ultrasonic irradiation and figuration of MPTS.

Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane. Publishing Authors By Initials

K Du,W Fu,R Wei,H Yang,J Xu,L Chang,Q Yu,G Zou,K Du,W Fu,R Wei,H Yang,J Xu,L Chang,Q Yu,G Zou,

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Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane. Journal Published:

PUBLICATION TYPE: Journal Article

Journal: Ultrasonics sonochemistry

VOLUME: 15

Page Numbers: 233-8

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ISSN: 1350-4177

DAY: 1

MONTH: 05

YEAR: 2007

Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane. Information

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LANGUAGE: eng

NlmUniqueID: 9433356

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Grant and Affiliation Information for Ultrasonic-assisted synthesis of highly dispersed MoO(3) nanospheres using 3-mercaptopropyltrimethoxysilane.

AFFILIATION: National Laboratory of Superhard Materials, Jilin University, Changchun, 130012 Jilin, PR China.

Country: Netherlands

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MEDLINETA: Ultrason Sonochem

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