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Towards automated diffraction tomography. Part II-Cell parameter determination.

Towards automated diffraction tomography. Part II-Cell parameter determination. Research Abstract Details 

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  • Towards automated diffraction tomography. Part II-Cell parameter determination. Abstract Text:

    Automated diffraction tomography (ADT) allows the collection of three-dimensional (3d) diffraction data sets from crystals down to a size of only few nanometres. Imaging is done in STEM mode, and diffraction data are collected with quasi-parallel beam nanoelectron diffraction (NED). Here, we present a set of developed processing steps necessary for automatic unit-cell parameter determination from the collected 3d diffraction data. Cell parameter determination is done via extraction of peak positions from a recorded data set (called the data reduction path) followed by subsequent cluster analysis of difference vectors. The procedure of lattice parameter determination is presented in detail for a beam-sensitive organic material. Independently, we demonstrate a potential (called the full integration path) based on 3d reconstruction of the reciprocal space visualising special structural features of materials such as partial disorder. Furthermore, we describe new features implemented into the acquisition part.

    Towards automated diffraction tomography. Part II-Cell parameter determination. Publishing Authors By Initials

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    PUBMED ID PMID:

    MEDLINE DATE:

    Towards automated diffraction tomography. Part II-Cell parameter determination. Journal Published:

    PUBLICATION TYPE: Journal Article

    Journal: Ultramicroscopy

    VOLUME: 108

    Page Numbers: 763-72

    Journal Abbreviation:

    ISSN: 0304-3991

    DAY: 12

    MONTH: 01

    YEAR: 2008

    Towards automated diffraction tomography. Part II-Cell parameter determination. Information

    Number of References:

    LANGUAGE: eng

    NlmUniqueID: 7513702

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    Grant and Affiliation Information for Towards automated diffraction tomography. Part II-Cell parameter determination.

    AFFILIATION: Institute of Physical Chemistry, Johannes Gutenberg-University, Welderweg 11, 55099 Mainz, Germany.

    Country: Netherlands

    Netherlands Research PublicationNetherlands Research Publication

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    MEDLINETA: Ultramicroscopy

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