Total synthesis of (-)-okilactomycin.

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Total synthesis of (-)-okilactomycin. Abstract Text:

Amos B Smith,Kallol Basu,Todd Bosanac,Amos B Smith,Kallol Basu,Todd Bosanac,Amos B Smith,Kallol Basu,Todd Bosanac,

A highly convergent synthesis of (-)-okilactomycin is described. Key reactions of this synthesis include a strategy-level diastereoselective oxy-Cope rearrangement/oxidation sequence, a Petasis-Ferrier union/rearrangement tactic, and an efficient RCM reaction to construct the 13-membered macrocyclic ring.

Total synthesis of (-)-okilactomycin. Publishing Authors By Initials

AB Smith,K Basu,T Bosanac,AB Smith,K Basu,T Bosanac,AB Smith,K Basu,T Bosanac,

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Total synthesis of (-)-okilactomycin. Journal Published:

PUBLICATION TYPE: Journal Article

Journal: Journal of the American Chemical Society

VOLUME: 129

Page Numbers: 14872-4

Journal Abbreviation: J. Am. Chem. Soc.

ISSN: 0002-7863

DAY: 13

MONTH: 11

YEAR: 2007

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LANGUAGE: eng

NlmUniqueID: 7503056

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Grant and Affiliation Information for Total synthesis of (-)-okilactomycin.

AFFILIATION: Department of Chemistry, Laboratory for Research on the Structure of Matter, and Monell Chemical Senses Center, University of Pennsylvania, Philadelphia, Pennsylvania 19104.

Country: United States