The decarboxylative blaise reaction.

The decarboxylative blaise reaction. Research Abstract Details 

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The decarboxylative blaise reaction. Abstract Text:

Jae Hoon Lee,Bo Seung Choi,Jay Hyok Chang,Hee Bong Lee,Joo-Yong Yoon,Jaeick Lee,Hyunik Shin,Jae Hoon Lee,Bo Seung Choi,Jay Hyok Chang,Hee Bong Lee,Joo-Yong Yoon,Jaeick Lee,Hyunik Shin,Jae Hoon Lee,Bo Seung Choi,Jay Hyok Chang,Hee Bong Lee,Joo-Yong Yoon,Jaeick Lee,Hyunik Shin,

Reaction of aryl nitriles with potassium ethyl malonate in the presence of zinc chloride and a catalytic amount of Hünig's base provided beta-amino acrylates in moderate to good yield. Compared to the classical Blaise reaction, this reaction is safer (endothermic), devoid of lachrymatory reagent, and is possible with 0.5-1.0 equiv of zinc chloride.

The decarboxylative blaise reaction. Publishing Authors By Initials

JH Lee,BS Choi,JH Chang,HB Lee,JY Yoon,J Lee,H Shin,JH Lee,BS Choi,JH Chang,HB Lee,JY Yoon,J Lee,H Shin,JH Lee,BS Choi,JH Chang,HB Lee,JY Yoon,J Lee,H Shin,

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The decarboxylative blaise reaction. Journal Published:

PUBLICATION TYPE: Journal Article

Journal: The Journal of organic chemistry

VOLUME: 72

Page Numbers: 10261-3

Journal Abbreviation: J. Org. Chem.

ISSN: 0022-3263

DAY: 30

MONTH: 11

YEAR: 2007

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LANGUAGE: eng

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Grant and Affiliation Information for The decarboxylative blaise reaction.

AFFILIATION: Chemical Development Division, LG Life Sciences, Ltd./R&D, 104-1, Moonji-dong, Yusong-gu, Daejeon 305-380, Korea hisin@lgls.com.

Country: United States

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MEDLINETA: J Org Chem

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