Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood.

Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Research Abstract Details 

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Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Abstract Text:

M Yamane,I Yanagisawa,

One of the authors reported previously on the presence of 1-methylheptyl gamma-bromoacetoacetate (MHBAA) in human cerebrospinal fluid. In this work, a microdetermination of MHBAA in human blood plasma was developed. The sulfhydryl group of 5-(dimethylamino)-1-naphthalene-sulfonyl L-cysteine (DANSYL L-cysteine) reacted with Br at the gamma-position of MHBAA to form a thioether bond, and a fluorescent derivative was obtained. The fluorescent derivative was separated by TLC. Quantitative determination of MHBAA was done by the radiodilution method combined with fluorometry. It was shown that MHBAA exists in human blood plasma at a concentration of several hundred pmol per ml.

Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Publishing Authors By Initials

M Yamane,I Yanagisawa,

For similar sulfhydryl compounds research abstracts see: sulfhydryl compounds research

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Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Journal Published:

PUBLICATION TYPE: Research Support, Non-U.S. Gov

Journal: Journal of biochemistry

VOLUME: 92

Page Numbers: 2009-20

Journal Abbreviation: J. Biochem.

ISSN: 0021-924X

DAY: 19

MONTH: Dec

YEAR: 1982

Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Information

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LANGUAGE: eng

NlmUniqueID: 376600

Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Keywords Mesh Terms:

KEYWORDS: Sulfhydryl Compounds

MESH TERMS: chemical synthesis

Chemical & Substance for Abstract: Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood. Information

Substance Name: 2-octyl-gamma-bromoacetoacetate

Registry Number: 40529-35-9

Grant and Affiliation Information for Microdetermination of 1-Methylheptyl gamma-bromoacetoacetate in human blood.

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Country: JAPAN

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MEDLINETA: J Biochem

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