Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography.
Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography. Research Abstract Details
Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography. Abstract Text:
pH-Zone-refining countercurrent chromatography was successfully applied to the separation of salvianolic acid B from the Chinese medicinal plant, Salvia miltiorrhiza Bunge, using a multilayer coil planet centrifuge. A 2.0 g quantity of sample was separated using the following two-phase solvent system: methyl tert-butyl ether (MtBE)-water, 10 mM TFA in organic stationary phase and 10 mM ammonia in aqueous mobile phase. The obtained fractions were analyzed by HPLC and ESI-MS. The separation yielded 572 mg of the main component of salvianolic acid B with a purity of 94.1%.
Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography. Publishing Authors By Initials
Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography. Journal Published:
PUBLICATION TYPE: Journal Article
Journal: Journal of separation science
VOLUME: 30
Page Numbers: 3214-7
Journal Abbreviation:
ISSN: 1615-9306
DAY: 17
MONTH: Dec
YEAR: 2007
Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography. Information
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LANGUAGE: eng
NlmUniqueID: 101088554
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Grant and Affiliation Information for Large-scale separation of salvianolic acid B from the Chinese medicinal plant Salvia miltiorrhiza by pH-zone-refining countercurrent chromatography.
AFFILIATION: Shandong Analysis and Test Center, Shandong Academy of Sciences, Jinan, Shandong, China. Fax: +86-531-8296-4889.
Country: Germany
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MEDLINETA: J Sep Sci
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