Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates.

Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Research Abstract Details 

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Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Abstract Text:

Kristina L Wade,Ian J Garrard,Jed W Fahey,

An improved hydrophilic interaction liquid chromatography (HILIC) method has been developed to separate members of a closely related family of chemoprotective phytochemicals called glucosinolates. This method exploits the emergence of a second generation of HILIC chemistry, using a silica-based permanently zwitterionic stationary phase. These columns are more robust, durable, and glucosinolates separations are more reproducible than with the original polyhydroxyethyl aspartamide columns. Furthermore, the HILIC system that we report herein permits much greater alteration of the mobile phase composition for customized separation of glucosinolates from plant extracts, across a wide spectrum of polarity.

Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Publishing Authors By Initials

KL Wade,IJ Garrard,JW Fahey,

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Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Journal Published:

PUBLICATION TYPE: Validation Studies

Journal: Journal of chromatography. A

VOLUME: 1154

Page Numbers: 469-72

Journal Abbreviation:

ISSN: 0021-9673

DAY: 20

MONTH: 04

YEAR: 2007

Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Information

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LANGUAGE: eng

NlmUniqueID: 9318488

Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Keywords Mesh Terms:

KEYWORDS: Imidoesters

MESH TERMS: analysis

Chemical & Substance for Abstract: Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates. Information

Substance Name: sinigrin

Registry Number: 534-69-0

Grant and Affiliation Information for Improved hydrophilic interaction chromatography method for the identification and quantification of glucosinolates.

AFFILIATION: Johns Hopkins School of Medicine, Department of Pharmacology and Molecular Sciences, Lewis B. and Dorothy Cullman Cancer Chemoprotection Center, 725 N. Wolfe Street, 406 WBSB, Baltimore, MD 21205, USA.

Country: Netherlands

AGENCY: United States NCI

GRANT: CA 93780-04

ACRONYM: CA

MEDLINETA: J Chromatogr A

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