An eight-position capillary sample spinning stage has been developed for use in conjunction with the versatile vacuum diffractometer (BIGDIFF) at BL20B at the Photon Factory. BIGDIFF is often used in its powder diffraction mode using powders mounted in capillaries and up to eight imaging plates to record the diffraction pattern from the sample. Using the multiple spinning stage a number of diffraction patterns can be recorded on the imaging plates if the imaging-plate cassette is moved behind the Weissenberg screen to a new position after exposure of the sample to the beam. Not only is this system more efficient in terms of time saved in the pumping-down process, but also it has the advantage of allowing the diffraction patterns of standards to be recorded, thereby calibrating both the angle scale of the diffractometer and the intensity scales of the imaging plates absolutely.
An eight-position capillary sample spinning stage for the diffractometer at BL20B at the Photon Factory. Publishing Authors By Initials
An eight-position capillary sample spinning stage for the diffractometer at BL20B at the Photon Factory. Journal Published:
PUBLICATION TYPE: Journal Article
Journal: Journal of synchrotron radiation
VOLUME: 5
Page Numbers: 823-5
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ISSN: 0909-0495
DAY: 1
MONTH: 05
YEAR: 1998
An eight-position capillary sample spinning stage for the diffractometer at BL20B at the Photon Factory. Information
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LANGUAGE: eng
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Grant and Affiliation Information for An eight-position capillary sample spinning stage for the diffractometer at BL20B at the Photon Factory.
AFFILIATION: Information Sciences and Engineering, University of Canberra, Belconnen, ACT 2616, Australia.
Country: Denmark
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MEDLINETA: J Synchrotron Radiat
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