Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction.

Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction. Research Abstract Details 

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Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction. Abstract Text:

Carlos del Pozo,Adam I Keller,Tadamichi Nagashima,Dennis P Curran,

A new fluorous carbodiimide is introduced along with a convenient procedure for amide coupling reactions. Reactions of acids and amines under standard conditions for carbodiimide couplings, followed by simple reverse fluorous solid-phase extraction (FSPE) over standard silica gel, provide the target amide products in good yields and purities. The use of HFE-7100 as a fluorous solvent is crucial for the success of the reverse FSPE.

Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction. Publishing Authors By Initials

C del Pozo,AI Keller,T Nagashima,DP Curran,

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Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction. Journal Published:

PUBLICATION TYPE: Research Support, N.I.H., Extr

Journal: Organic letters

VOLUME: 9

Page Numbers: 4167-70

Journal Abbreviation: Org. Lett.

ISSN: 1523-7060

DAY: 21

MONTH: 09

YEAR: 2007

Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction. Information

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LANGUAGE: eng

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Grant and Affiliation Information for Amide bond formation with a new fluorous carbodiimide: separation by reverse fluorous solid-phase extraction.

AFFILIATION: Department of Chemistry, University of Pittsburgh, Pittsburgh, Pennsylvania 15260, USA.

Country: United States

AGENCY: United States NIGMS

GRANT: R44GM067326

ACRONYM: GM

MEDLINETA: Org Lett

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