A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines.

A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines. Research Abstract Details 

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A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines. Abstract Text:

Alexey Potapov,Boris Epel,Daniella Goldfarb,Alexey Potapov,Boris Epel,Daniella Goldfarb,

A new, triple resonance, pulse electron paramagnetic resonance (EPR) sequence is described. It provides spin links between forbidden electron spin transitions (DeltaM(S)=+/-1, DeltaM(I) not equal0) and allowed nuclear spin transitions (DeltaM(I)=+/-1), thus, facilitating the assignment of nuclear frequencies to their respective electron spin manifolds and paramagnetic centers. It also yields the relative signs of the hyperfine couplings of the different nuclei. The technique is based on the combination of electron-nuclear double resonance (ENDOR) and electron-electron double resonance (ELDOR)-detected NMR experiments in a way similar to the TRIPLE experiment. The feasibility and the information content of the method are demonstrated first on a single crystal of Cu-doped L-histidine and then on a frozen solution of a Cu-histidine complex.

A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines. Publishing Authors By Initials

A Potapov,B Epel,D Goldfarb,A Potapov,B Epel,D Goldfarb,

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A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines. Journal Published:

PUBLICATION TYPE: Journal Article

Journal: The Journal of chemical physics

VOLUME: 128

Page Numbers: 052320

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ISSN: 0021-9606

DAY: 7

MONTH: Feb

YEAR: 2008

A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines. Information

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LANGUAGE: eng

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Grant and Affiliation Information for A triple resonance hyperfine sublevel correlation experiment for assignment of electron-nuclear double resonance lines.

AFFILIATION: Chemical Physics Department, Weizmann Institute of Science, Rehovot 76100, IsraelDepartment of Radiation and Cellular Oncology, MC1105 The University of Chicago Medical Center, Chicago, Illinois 60637, USA.

Country: United States

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MEDLINETA: J Chem Phys

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