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to attach Boc protected group...

to attach Boc protected group... - Peptide Forum

to attach Boc protected group... - Peptide Forum. Ask and discuss questions on peptide protocols, custom peptide synthesis, peptide identification and peptide sequencing.


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  #1  
Old 05-18-2011, 03:37 PM
Pipette Filler
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Default to attach Boc protected group...



Hey!

I have a peptide and I want to change the Fmoc group to the Boc group....

Fmoc-Nle-Ser-Pro....Wang Resin....

to cleavage Fmoc I know that I could do it with piperadine in DMF...what about to attach Boc? Boc2O and TEA? and in which solvent could work better? DMF? THF?

Thanks!
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Old 06-06-2011, 09:57 AM
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Default Re: to attach Boc protected group...

In THF or DCM using Boc Anhydride (Monitor by Kaiser Test)
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Old 06-06-2011, 10:00 AM
Kunal Pandya's Avatar
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Thumbs up Re: to attach Boc protected group...

In THF or DCM using Boc Anhydride (Monitor by Kaiser Test)

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Kunal Pandya
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